Logo-apb
Adv Pharm Bull. 2017;7(2): 329-334.
doi: 10.15171/apb.2017.039
PMID: 28761836
PMCID: PMC5527248
Scopus ID: 85021456264
  Abstract View: 2287
  PDF Download: 1418

Short Communication

Study of Thermal Analysis Behavior of Fenbendazole and Rafoxanide

Ali Kamal Attia 1*, Ahmed Sayed Saad 2, Manal Sami Alaraki 1, Eman Saad Elzanfaly 2

1 National Organization for Drug Control and Research, P.O. Box 29, Cairo, Egypt.
2 Analytical Chemistry Department, Faculty of Pharmacy, Cairo University, Kasr El-Aini Street, Cairo, Egypt.
*Corresponding Author: Email: alikamal1978@hotmail.com

Abstract

Purpose: Thermal analysis techniques have been applied to study the thermal behavior of fenbendazole (Fen) and rafoxanide (Raf). Semi-empirical molecular orbital calculations were used to confirm these results.

Methods: Thermogravimetric analysis, derivative thermogravimetry, differential thermal analysis and differential scanning calorimetry were used to determine the thermal behavior and purity of the drugs under investigation.

Results: Thermal behavior of Fen and Raf were augmented using semi-empirical molecular orbital calculations. The purity values were found to be 99.17% and 99.60% for Fen and Raf, respectively.

Conclusion: Thermal analysis techniques gave satisfactory results to obtain quality control parameters such as melting point and degree of purity at low cost, furthermore, its simplicity and sensitivity justifies its application in quality control laboratories.




First Name
Last Name
Email Address
Comments
Security code


Abstract View: 2263

Your browser does not support the canvas element.


PDF Download: 1418

Your browser does not support the canvas element.

Submitted: 03 Jan 2017
Revision: 18 May 2017
Accepted: 20 May 2017
ePublished: 30 Jun 2017
EndNote EndNote

(Enw Format - Win & Mac)

BibTeX BibTeX

(Bib Format - Win & Mac)

Bookends Bookends

(Ris Format - Mac only)

EasyBib EasyBib

(Ris Format - Win & Mac)

Medlars Medlars

(Txt Format - Win & Mac)

Mendeley Web Mendeley Web
Mendeley Mendeley

(Ris Format - Win & Mac)

Papers Papers

(Ris Format - Win & Mac)

ProCite ProCite

(Ris Format - Win & Mac)

Reference Manager Reference Manager

(Ris Format - Win only)

Refworks Refworks

(Refworks Format - Win & Mac)

Zotero Zotero

(Ris Format - Firefox Plugin)