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Adv Pharm Bull. 2023;13(3): 592-600.
doi: 10.34172/apb.2023.064
PMID: 37646058
PMCID: PMC10460804
  Abstract View: 566
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Research Article

Expression, Purification and Characterization of Functional Teduglutide Using GST Fusion System in Prokaryotic Cells

Ali Akbar Alizadeh 1 ORCID logo, Saba Rasouli 2,3 ORCID logo, Omid Jamshidi Kandjani 1 ORCID logo, Salar Hemmati 4 ORCID logo, Siavoush Dastmalchi 1,3,5* ORCID logo

1 Biotechnology Research Center, Tabriz University of Medical Sciences, Tabriz, Iran.
2 Pharmaceutical Analysis Research Center, Tabriz University of Medical Sciences, Tabriz, Iran.
3 School of Pharmacy, Tabriz University of Medical Sciences, Tabriz, Iran.
4 Drug Applied Research Center, Tabriz University of Medical Sciences, Tabriz, Iran.
5 Faculty of Pharmacy, Near East University, Po.Box: 99138, Nicosia, North Cyprus, Mersin 10, Turkey.
*Corresponding Author: Siavoush Dastmalchi, Emails: dastmalchi.s@tbzmed.ac.ir; , Email: siavoush11@yahoo.com

Abstract

Purpose: Teduglutide is the first and only FDA-approved drug for long-term treatment of short bowel syndrome (SBS). The current study aimed to present an approach for production of teduglutide using recombinant DNA technology.

Methods: The coding gene for teduglutide was cloned into pGEX-2T vector, where coding sequence for factor Xa cleavage site was added between GST and teduglutide coding genes. The GST-teduglutide protein was overexpressed in E. coli BL21 (DE3) strain and affinity purified using glutathione sepharose affinity column.

Results: On-column proteolytic activity of factor Xa followed by size exclusion chromatography resulted in the pure teduglutide. Circular dichroism (CD) spectropolarimetry showed that the produced teduglutide folds into mainly α-helical structure (>50%), as expected. In mass spectroscopy analysis, the fragments of teduglutide resulted by cyanogen bromide cleavage as well as those expected theoretically due to mass fragmentation were identified. The functionality of the produced peptide was evaluated by measuring its proliferative effect on Caco2 intestinal epithelial cells, and the results indicated that produced teduglutide induces cell proliferation by 19±0.30 and 33±7.82 % at 1.21 and 3.64 µM concentrations, respectively, compared to untreated cells.

Conclusion: Teduglutide was successfully expressed and purified and its functionality and structural integrity were confirmed by in vitro experiments. We believe that the experimental-scale method presented in the current study can be useful for pilot-scale and also industrial-scale production of teduglutide.

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Submitted: 28 May 2022
Revision: 15 Nov 2022
Accepted: 04 Dec 2022
ePublished: 06 Dec 2022
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